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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1175400Generated: November 1, 2026

Methanesulfonamide → HCID 59558824, compound

https://huagongshe.com/reaction/1175400

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanesulfonamideHCID 72879—
Reactant4-Chloro-2-([(2,3-difluorophenyl)methyl]thio]-6-methoxypyrimidineHCID 86619877—
ProductHCID 59558824HCID 59558824—

Reaction Steps

The title compound was prepared from methane sulfonamide (0.11 g) and 4-Chloro-2-[[(2,3-difluorophenyl)methyl]thio]-6-methoxypyrimidine (the product of Example 35, step i) (0.25 g) according to the procedure outlined in Example 1, step iv). The crude material was purified by column chromatography using EtOAc/isohexane (2:8) as eluent. Yield: 0.12 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07838675B2
Source datasetuspto-grants-2010_11
ORD IDord-ce5896d32854479e97637f14e0265c09
Source noteuspto-grants-2010_11