HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylamine → HCID 58789413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | ([1,1'-Biphenyl]-4-yl)[(tert-butoxycarbonyl)amino]acetic acid | HCID 18770129 | — |
| Product | HCID 58789413 | HCID 58789413 | 55% |
Reaction Steps
Prepared in a similar manner to Example 20 from 2-(biphenyl-4-yl)-2-(tert-butoxycarbonylamino)acetic acid and isobutyl amine. Yield: 55%. 1H NMR (400 MHz, dMSO): δ 0.76-0.78 (d, 6H), 1.38 (s, 9H), 1.63-1.66 (m, 1H), 2.84-2.92 (m, 2H), 5.30-5.22 (d, 1H), 7.25-7.27 (d, 1H), 7.35-7.37 (m, 1H), 7.43-7.51 (m, 4H), 7.61-7.66 (m, 4H), 8.14-8.17 (t, 1H); MS+H (383).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842324B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-966dfc33799141b1a424bfca06389b6f |
| Source note | uspto-grants-2010_11 |