((2R,3S,4R,5R)-5-(6-amino-9H-purin-9-yl)-3,4-dihydroxy-2-methyl-tetrahydrofuran-2-yloxy)methylphosphonic acid → HCID 25006013, compound

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Reaction Steps

Compound 32.4 (61 mg, 75% yield) was synthesized from compound 32.2 (95 mg, 0.24 mmol) using the procedure described for the preparation of compound 31.5. 1H NMR (300 MHz, D2O) δ 1.38 (s, 3H), 3.50 (m, 2H), 3.98 (d, 1H, J=4.6), 5.84 (d, 1H, J=7.6), 6.08 (d, 1H, J=7.3), 7.81 (d, 1H, J=8.2). LRMS [M-H]− C10H15N2O9P requires 337.2. Found 337.2.

Provenance & Evidence