Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 1H-Indazol-4-amine, 1-methyl- | HCID 153838 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66745445 | HCID 66745445 | — |
Reaction Steps
A solution of phenyl chloroformate (1.1 mmol) in chloroform was cooled to 0° C. 1-methyl-1H-indazole-4-amine in dry THF was added to the reaction mixture dropwise at 0° C. Pyridine (1 mmol) was added to the reaction mixture. Reaction mixture was stirred at 0° C. for 30 minutes and was then stirred at room temperature for 15 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07842703B2 |
|---|
| Source dataset | uspto-grants-2010_11 |
|---|
| ORD ID | ord-bee261ee171c4786982ab29202cadd3c |
|---|
| Source note | uspto-grants-2010_11 |
|---|
