HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57498037, compound → 5-Phenyluracil
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57498037 | HCID 57498037 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 5-Phenyluracil | HCID 287110 | 80% |
Reaction Steps
2,4-Dimethoxy-5-phenyl-pyrimidine was suspended in 6N HCl and heated to 100 C for 24 h. Solution was cooled in an ice bath to afford title compound as a white solid 119 mg (80% yield). HNMR (500 MHz, dmso): 111.25 (1H, s), 11.15 (1H, d), 7.65 (1H, d), 7.55 (2H, d), 7.35 (2H, m), 7.25 (1H, t).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842712B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-8668a78e75e24d279c8e1c721e694c29 |
| Source note | uspto-grants-2010_11 |