HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanuric chloride → HCID 178478357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanuric chloride | HCID 7954 | — |
| Reactant | HCID 178507266 | HCID 178507266 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178478357 | HCID 178478357 | 50.4% |
Reaction Steps
A solution of 5-Cyclopropyl-2H-pyrazol-3-ylamine (334 mg, 2.71 mmol) in 2 ml of THF was added dropwise to a solution of 2,4,6-Trichloro-[1,3,5]triazine (500 mg, 2.71 mmol) in 5 ml of THF at room temperature. After 1 hour, the precipitate was collected to afford 370 mg (50.4% yield) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842712B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-f064491415da43cb924994cf14229aac |
| Source note | uspto-grants-2010_11 |