HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 15895594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 4-Aminobenzyl alcohol | HCID 69331 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15895594 | HCID 15895594 | — |
Reaction Steps
A solution of 3.75 g 4-aminobenzylalcohol and 3.3 ml isocyanato-benzene in 120 ml dichloromethane was stirred at 23° C. for 2 hours. Afterwards, the reaction mixture was filtered. The crystalline product was washed with diethylether. 6.82 g product was obtained which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842809B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-3a098eda71ea48f298c7dad8b749d6ab |
| Source note | uspto-grants-2010_11 |