HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → HCID 58751679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | Methyl cyanoacetate | HCID 7747 | — |
| Reactant | 3-Methyl-2-butanone | HCID 11251 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Product | HCID 58751679 | HCID 58751679 | — |
Reaction Steps
In analogy to the procedure described for Example 3a, reaction of 61.7 g ammonium acetate, 10.67 mL methyl cyanoacetate, 10.71 mL 3-methyl-butan-2-one, and 15.12 g 4-nitrobenzaldehyde yielded 4.24 g product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842809B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-71f1d80c6b3d4a3a925243d966233749 |
| Source note | uspto-grants-2010_11 |