1,3-Dibromopropane → HCID 63269422, compound

HRID 1176439Notes

Reaction equation

HRID 1176439 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([F:8])=[CH:4][C:3]=1[OH:9].[Br:10][CH2:11][CH2:12][CH2:13]Br>>[Br:10][CH2:11][CH2:12][CH2:13][O:9][C:3]1[CH:4]=[C:5]([F:8])[CH:6]=[CH:7][C:2]=1[F:1]

Participants

3

Reactant 2

HCID 80011,3-DibromopropaneHCID 949522,5-Difluorophenol

Product 1

HCID 63269422HCID 63269422, compound

Procedure

Analogously to Example 91b, 1.40 g of 2,5-difluorophenol and 21.5 g of 1,3-dibromopropane are reacted. The title compound is obtained as a colourless oil. Rf=0.59 (1:3 EtOAc-heptane); Rt=4.84.

Sources & evidence

ORD record
ord-be3f552cd6f64216a97fdcb44850b745
Source dataset
uspto-grants-2010_11
Patent number
US07842688B2

Reaction notes

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