HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromopropane → 2-(3-Bromopropoxy)-1,3-difluorobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | 2,6-Difluorophenol | HCID 94392 | — |
| Product | 2-(3-Bromopropoxy)-1,3-difluorobenzene | HCID 68500425 | — |
Reaction Steps
Analogously to Example 91b, 2.00 g of 2,6-difluorophenol and 30.7 g of 1,3-dibromopropane are reacted. The title compound is obtained as a colourless oil. Rf=0.70 (1:6 EtOAc-heptane); Rt=4.97.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-5cad48b84bbf45818995d9427d545ce5 |
| Source note | uspto-grants-2010_11 |