1,3-Dibromopropane → HCID 62784847, compound

HRID 1176487Notes

Reaction equation

HRID 1176487 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[C:6]([F:8])[CH:7]=1.[Br:10][CH2:11][CH2:12][CH2:13]Br>>[Br:10][CH2:11][CH2:12][CH2:13][O:9][C:4]1[CH:3]=[C:2]([F:1])[CH:7]=[C:6]([F:8])[CH:5]=1

Participants

3

Reactant 2

HCID 80011,3-DibromopropaneHCID 759283,5-Difluorophenol

Product 1

HCID 62784847HCID 62784847, compound

Procedure

Analogously to Example 91b, 0.98 g of 3,5-difluorophenol and 15.2 g of 1,3-dibromopropane are reacted. The title compound is obtained as a colourless oil. Rf=0.70 (1:6 EtOAc-heptane); Rt=5.13.

Sources & evidence

ORD record
ord-f89c952ec92f4e0f9eb9016a13fd0c48
Source dataset
uspto-grants-2010_11
Patent number
US07842688B2

Reaction notes

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