HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 3-hydroxy-4-(4-hydroxyphenyl)piperidinecarboxylate → HCID 68499094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 3-hydroxy-4-(4-hydroxyphenyl)piperidinecarboxylate | HCID 68500730 | — |
| Reactant | HCID 86626135 | HCID 86626135 | — |
| Product | HCID 68499094 | HCID 68499094 | — |
Reaction Steps
Analogously to Method I, 9.170 g of benzyl 3-hydroxy-4-(4-hydroxyphenyl)piperidinecarboxylate and 11.00 g of tert-butyl 3-(toluenesulphonyloxy)azetidine-1-carboxylate are reacted. The title compound is obtained as a yellow oil. Rf=0.23 (3:1 EtOAc-heptane); Rt=5.01.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-f907f71be235418e881a16fd3f496a5c |
| Source note | uspto-grants-2010_11 |