HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzimidazole → HCID 11573841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzimidazole | HCID 13624 | — |
| Reactant | 4-Fluorobenzyl bromide | HCID 68021 | — |
| Product | HCID 11573841 | HCID 11573841 | — |
Reaction Steps
The title compound was prepared from 2-aminobenzimidazole and 4-fluorobenzyl bromide by Procedure A. The product was isolated by preparative LCMS to give the title compound as the free base (white solid, mp 148-150° C.). MS(ES+) m/z 351 ([M+1]+, 100). 1NMR (DMSO-d6) δ 5.07 (s, 4H), 5.75 (br s, 1H), 6.78-6.91 (m, 4H), 7.12-7.18 (m, 4H), 7.30-7.42 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842817B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-4fce2fc7e2b54fcabc404f12fcbe0b30 |
| Source note | uspto-grants-2010_11 |