HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzimidazole → HCID 11689553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzimidazole | HCID 13624 | — |
| Reactant | 4-(Bromomethyl)-1,2-difluorobenzene | HCID 581436 | — |
| Product | HCID 11689553 | HCID 11689553 | — |
Reaction Steps
The title compound was prepared from 2-aminobenzimidazole and 3,4-difluorobenzyl bromide by Procedure A. The product was isolated by preparative LCMS to give the title compound as the free base (white solid, mp 114-117° C.). MS(ES+) m/z 387 ([M+1]+, 100). 1NMR (DMSO-d6) δ 5.08 (br s, 4H), 5.86 (br s, 1H), 6.72-6.96 (m, 4H), 7.05-7.22 (m, 2H), 7.35-7.45 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842817B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-5f6bf46f35294e288f422309808efc50 |
| Source note | uspto-grants-2010_11 |