HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → N-ethyl-2-nitrobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 2-Nitrobenzenesulfonyl chloride | HCID 15540 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-ethyl-2-nitrobenzenesulfonamide | HCID 744706 | — |
Reaction Steps
2-nitrobenzenesulfonyl chloride (10 g) is added portion-wise to 70% ethylamine in water at 0-5° C., maintaining the temperature. It is stirred for 15 minutes until completing the transformation. Water (80 mL) is added, maintaining the temperature. It is stirred for 30 minutes. It is filtered, washed and dried, obtaining 8.97 g of N-ethyl-2-nitrobenzenesulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842821B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-19a61b390a364cd58f8acbef0d875aa7 |
| Source note | uspto-grants-2010_11 |