HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → HCID 22320427, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 22320469 | HCID 22320469 | — |
| Product | HCID 22320427 | HCID 22320427 | 78.9% |
Reaction Steps
Using the general method of Example 21 Part D, N-(2-chloroethyl)-3-nitroquinolin-4-amine (6.0 g, 23.84 mmol) was reacted with sodium thiomethoxide (2.11 g of 95%, 28.61 mmol) to provide 4.95 g of N-[2-(methylthio)ethyl]-3-nitroquinolin-4-amine as a dull yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07276515B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-2c06f0ca7b11426f81252e1ffda81f80 |
| Source note | uspto-grants-2007_10 |