HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22320435, compound → HCID 10237336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22320435 | HCID 22320435 | — |
| Reactant | HCID 178418793 | HCID 178418793 | — |
| Product | HCID 10237336 | HCID 10237336 | 80.1% |
Reaction Steps
Using the general method of Example 20 Part A, 1-(chlorobutyl)-2-ethyl-1H-imidazo[4,5-c]quinolin-4-amine (1.0 g, 3.30 mmol) was reacted with 2-mercaptopyrimidine (0.59 g, 5.3 mmol) to provide 1.0 g of 2-ethyl-1-[4-(pyrimidin-2-ylthio)butyl]-1H-imidazo[4,5-c]quinolin-4-amine as an off white powder, m.p. 182-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07276515B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-d77e1befac2d4778b9b851de9b4761b6 |
| Source note | uspto-grants-2007_10 |