Trimethylsilyl iodide → HCID 131726615, compound

Participants

Reaction Steps

Add 0.14 μl of iodotrimethylsilane to a solution, at ambient temperature, of 0.1 mmol of the compound of Example 11 in 1 ml of chloroform. The reaction mixture is stirred at ambient temperature for 5 minutes and then evaporated to dryness under reduced pressure. Chromatography over silica gel (dichloromethane/methanol:85/15) allows the expected product to be isolated.

Provenance & Evidence