N-Ethylaniline → HCID 23117587, compound

HRID 1178344Notes

Reaction equation

HRID 1178344 reaction equation
[CH2:1]([NH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[CH3:2].[C:10](Cl)(=[O:14])[C:11]([Cl:13])=[O:12]>C1(C)C=CC=CC=1>[CH2:1]([N:3]([C:10](=[O:14])[C:11]([Cl:13])=[O:12])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[CH3:2]

Participants

4

Reactant 2

HCID 7670N-EthylanilineHCID 65578Oxalyl chloride

Product 1

HCID 23117587HCID 23117587, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Similar to Referential Example 1, N-ethylaniline (1.0 g) was dissolved in toluene (10 mL), and oxalyl chloride (4.0 mL) was added thereto under cooling with ice. The temperature of the mixture was then returned to room temperature, and the mixture was stirred for 1 hour. The reaction mixture was concentrated under reduced pressure, to thereby give the title compound (2.05 g) as a brown oil. The compound was used without further purification.

Workup

  1. temperatureunder cooling with ice
  2. customwas then returned to room temperature
  3. concentrationThe reaction mixture was concentrated under reduced pressure

Sources & evidence

ORD record
ord-890c8dfb0c474547b2ada87948e05006
Source dataset
uspto-grants-2007_10
Patent number
US07276511B2

Reaction notes

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