Indole → HCID 68486842, compound

HRID 1178714Notes

Reaction equation

[CH:1]1[C:14]2[C:5](=[N:6][CH:7]=[C:8]3[C:13]=2[CH:12]=[CH:11][CH:10]=[CH:9]3)[CH:4]=[CH:3][CH:2]=1.[C:15]1([C:25](Cl)=[O:26])[C:24]2[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH:18]=[CH:17][CH:16]=1.[NH:28]1[C:36]2[C:31](=[CH:32][CH:33]=[CH:34][CH:35]=2)[CH:30]=[CH:29]1>>[NH:28]1[C:36]2[C:31](=[CH:32][CH:33]=[CH:34][CH:35]=2)[C:30]([CH:7]2[C:8]3[C:13](=[CH:12][CH:11]=[CH:10][CH:9]=3)[C:14]3[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=3[N:6]2[C:25]([C:15]2[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[CH:18]=[CH:17][CH:16]=2)=[O:26])=[CH:29]1

Participants

Reactant 3

HCID 798Indole

HCID 9189Phenanthridine

HCID 701461-Naphthalenecarbonyl chloride

Product 1

HCID 68486842HCID 68486842, compound

Procedure

[6-(1H-Indol-3-yl)-6H-phenanthridin-5-yl]-naphthalen-1-yl-methanone was prepared from phenanthridine, 1-naphthoyl chloride, and indole according to GP 2. Yield, 2%. (+)-ESI-MS: m/z=451 [M+H]+, 334 [M-indole+H]+.

Workup

customYield

Sources & evidence

ORD record: ord-17387085eeb3486f9cecb71b7676f83b
Source dataset: uspto-grants-2007_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07276606B2

Reaction notes

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