HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68526195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Tert-butyl 3-cyclohexyl-3-[(methylthio)methyl]-8-azabicyclo[3.2.1]octane-8-carboxylate | HCID 58695800 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68526195 | HCID 68526195 | — |
Reaction Steps
To a solution of 4.0 N HCl in dioxane (20.0 mL) was added tert-butyl 3-cyclohexyl-3-[(methylthio)methyl]-8-azabicyclo[3.2.1]octane-8-carboxylate (3-5) (0.870 g, 2.46 mmol). The mixture was stirred at room temperature for three hours and the volatiles were removed under vacuum to give (3-6) as a pale solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07276520B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-1277d9c0b5654b00b094e10817c71cc9 |
| Source note | uspto-grants-2007_10 |