HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22245967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 9922658 | HCID 9922658 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 22245967 | HCID 22245967 | — |
Reaction Steps
As described for example 1, 1.01 g of the polar diastereomer of N′-benzyl-N,N-dimethyl-1-phenyl-cyclohexane-1,4-diamine were also obtained, and were converted into 781 mg of the corresponding hydrochloride by dissolving in 8.1 ml 2-butanone and addition of 32.5 μl water followed by 457 μl chlorotrimethylsilane and stirring overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07276518B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-985ee61c9d9a478dbef2f793d7d5d5a9 |
| Source note | uspto-grants-2007_10 |