HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 69337912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | HCID 10156333 | HCID 10156333 | — |
| Solvent | HCID 22381885 | HCID 22381885 | — |
| Product | HCID 69337912 | HCID 69337912 | — |
Reaction Steps
As described for example 66, 129 mg of the polar diastereomer of N′-[2-(1H-indol-3-yl)-ethyl]-N,N,N′-trimethyl-1-phenyl-cyclohexane-1,4-diamine were also obtained and were converted into the corresponding dihydrochloride while warm in 2-butanone/acetone (15 ml/3 ml) with chlorotrimethylsilane (121 μl) (white solid; 141 mg; m.p. 198-206° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07276518B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-dfd34d675aa94d638485eef331693edf |
| Source note | uspto-grants-2007_10 |