HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86591660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86591662 | HCID 86591662 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86591660 | HCID 86591660 | — |
Reaction Steps
Analogously to Example II, the tert-butyl ester (Example IX) in glacial acetic acid was cleaved using 4N HCl in dioxane. After stripping off the solvent, the residue was dissolved in water, clarified with active carbon and then lyophilized; 0.72 g of white amorphous residue; ESI-MS [M+H+]: 450.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279468B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-5428248e84094ce0bc6d07d385d287da |
| Source note | uspto-grants-2007_10 |