Sodium Hydroxide → HCID 58978028, compound

Participants

Reaction Conditions

Reaction Steps

The product of Example 14 (4.5 g) was treated with 6 M HCl (50 mL), heated to 100° C. for 90 min, and then cooled to room temperature. The resulting solution was basified with 10% aqueous NaOH to pH 11, and extracted with DCM (3×5 mL). The combined extracts were dried (MgSO4), and concentrated under reduced pressure, giving the title compound as a brown gummy solid (4.3 g).

Provenance & Evidence