HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic anhydride → HCID 22047951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic anhydride | HCID 7922 | — |
| Reactant | 6-Methoxy-3-pyridinylamine | HCID 81121 | — |
| Product | HCID 22047951 | HCID 22047951 | — |
Reaction Steps
A mixture of 5-amino-2-methoxypyridine (1.24 g, 10.0 mmol) and succinic anhydride (1.00 g, 10.0 mmol) was heated with a heat gun for 10 minutes. After cooling to room temperature the product was purified by flash column chromatography (SiO2, ethyl acetate:acetone 25:75). Evaporation of the solvent yielded the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-0cb5bcb87a574e8596cb7477b50c5c6d |
| Source note | uspto-grants-2007_10 |