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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1179710Generated: October 30, 2026

Carbamic chloride, N-methyl-N-phenyl- → HCID 10308410, compound

https://huagongshe.com/reaction/1179710

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCarbamic chloride, N-methyl-N-phenyl-HCID 77969—
Reactantp-Tert-butoxyphenolHCID 2773621—
SolventDichloromethaneHCID 6344—
ProductHCID 10308410HCID 10308410—

Reaction Steps

The title compound was prepared from 4-tert-butoxy-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (Quad12/25, flash 12, dichloromethane) followed by a recrystallization from ethanol (41%, crystals). HPLC-MS m/z=300.3 (M+1), Rt: 4.7 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07279470B2
Source datasetuspto-grants-2007_10
ORD IDord-95573624b0204f8db0d77f20a4154d87
Source noteuspto-grants-2007_10