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HRID1179723

反应详情

EQUATION

反应方程式

HRID 1179723 的结构方程式

REACTANTS

反应物

2
结构：CN(C(=O)Cl)c1ccccc1
HCID77969

Carbamic chloride, methylphenyl-

C8H8ClNO

结构：O=[N+]([O-])c1ccc(Oc2ccc(O)cc2)cc1
HCID152450

4-(4-Nitrophenoxy)phenol

C12H9NO4

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(Oc2ccc([N+](=O)[O-])cc2)cc1)c1ccccc1
HCID10215649

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-nitro-phenoxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (71%, white crystals). HPLC-MS m/z=365.0 (M+1), Rt: 4.83 min. 4(300 MHz; CDCl3): 3.44 (s, 3H), 7.00 (d, 2H), 7.06 (d, 2H), 7.26-7.32 (m, 1H), 7.33-7.49 (m, 4H), 8.20 (dt, 2H).