Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1179724Generated: November 1, 2026

Carbamic chloride, N-methyl-N-phenyl- → HCID 10172359, compound

https://huagongshe.com/reaction/1179724

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCarbamic chloride, N-methyl-N-phenyl-HCID 77969—
Reactant4-(heptylsulfanyl)phenolHCID 3614283—
ProductHCID 10172359HCID 10172359—

Reaction Steps

The title compound was prepared from 4-heptylsulfanyl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (74%, colourless oil, HPLC-MS m/z=358.2 (M+1), Rt: 6.21 min. δH (200 MHz; CDCl3): 0.87 (t, 3H), 1.15-1.50 (m, 8H), 1.50-1.75 (m, 2H), 2.86 (t, 2H), 3.41 (s, 3H), 7.04 (d, 2H), 7.15-7.50 (m, 7H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07279470B2
Source datasetuspto-grants-2007_10
ORD IDord-af683eac36fd48f88a362fcb265bc709
Source noteuspto-grants-2007_10