huagongshe.com
HRID1179760

反应详情

EQUATION

反应方程式

HRID 1179760 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1
HCID155241

4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenol

C12H8F3NO2

结构：C[n+]1ccn(C(=O)N2CCc3ccccc3C2)c1.[I-]
HCID22047918

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1)N1CCc2ccccc2C1
HCID23635514

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenol and 3-(3,4-dihydro-1H-isoquinoline-2-carbonyl)-1-methyl-3H-imidazol-1-ium iodide. The crude product was recrystallized (ethanol) (53%). HPLC-MS m/z=415.2 (M+1), Rt: 5.3 min.

WORKUP

后处理

  1. customThe crude product was recrystallized (ethanol) (53%)