4-Pentylphenol → Methyl-phenyl-carbamic acid 4-pentyl-phenyl ester

HRID 1179792Notes

Reaction equation

HRID 1179792 reaction equation
[CH2:1]([C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[CH3:13][N:14]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:15](Cl)=[O:16]>>[CH2:1]([C:6]1[CH:7]=[CH:8][C:9]([O:12][C:15](=[O:16])[N:14]([CH3:13])[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 2

HCID 269754-PentylphenolHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 69517564Methyl-phenyl-carbamic acid 4-pentyl-phenyl ester

Procedure

The title product was prepared from 4-pentylphenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (4%, light brown oil). HPLC-MS: m/z=298.2 (M+1); Rt: 5.61 min.

Sources & evidence

ORD record
ord-54267d3b63dc4a718b2ccce14db1adf6
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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