HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pentylphenol → Methyl-phenyl-carbamic acid 4-pentyl-phenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pentylphenol | HCID 26975 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic acid 4-pentyl-phenyl ester | HCID 69517564 | — |
Reaction Steps
The title product was prepared from 4-pentylphenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (4%, light brown oil). HPLC-MS: m/z=298.2 (M+1); Rt: 5.61 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-54267d3b63dc4a718b2ccce14db1adf6 |
| Source note | uspto-grants-2007_10 |