Carbamic chloride, N-methyl-N-phenyl- → HCID 69519372, compound

HRID 1179793Notes

Reaction equation

HRID 1179793 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1.[CH3:12][N:13]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[C:14](Cl)=[O:15]>>[CH3:1][O:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][C:8]([O:11][C:14](=[O:15])[N:13]([CH3:12])[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:7][CH:6]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 925164-(2-Methoxyethyl)phenol

Product 1

HCID 69519372HCID 69519372, compound

Procedure

The title product was prepared from 4-(2-methoxyethyl)phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (4%, light yellow oil). HPLC-MS: m/z=286.1 (M+1); Rt: 4.01 min.

Sources & evidence

ORD record
ord-4c7757ebc31e493ebe4813e0d9e506d7
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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