3-Hydroxypyridine → HCID 69518876, compound

HRID 1179796Notes

Reaction equation

HRID 1179796 reaction equation
[OH:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=1.[CH3:8][N:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:10](Cl)=[O:11]>>[N:4]1[CH:5]=[CH:6][CH:7]=[C:2]([O:1][C:10](=[O:11])[N:9]([CH3:8])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:3]=1

Participants

3

Reactant 2

HCID 79713-HydroxypyridineHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 69518876HCID 69518876, compound

Procedure

The title product was prepared from 3-hydroxypyridine and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (94%, colourless oil).

Sources & evidence

ORD record
ord-b797484e1ffc4fa3879a3d4d33501adc
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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