3-Phenoxyphenol → Methyl-phenyl-carbamic Acid 3-phenoxy-phenyl Ester

HRID 1179798Notes

Reaction equation

HRID 1179798 reaction equation
[O:1]([C:8]1[CH:9]=[C:10]([OH:14])[CH:11]=[CH:12][CH:13]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:15][N:16]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:17](Cl)=[O:18]>>[O:1]([C:8]1[CH:9]=[C:10]([O:14][C:17](=[O:18])[N:16]([CH3:15])[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:11]=[CH:12][CH:13]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 128423-PhenoxyphenolHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 69519068Methyl-phenyl-carbamic Acid 3-phenoxy-phenyl Ester

Procedure

The title product was prepared from 3-phenoxyphenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (79%, colourless oil). HPLC-MS: m/z=320.1 (M+1); Rt: 5.16 min.

Sources & evidence

ORD record
ord-e85b1339889e4b08ae6bee14ab28be75
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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