HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenoxyphenol → Methyl-phenyl-carbamic Acid 3-phenoxy-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenoxyphenol | HCID 12842 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic Acid 3-phenoxy-phenyl Ester | HCID 69519068 | — |
Reaction Steps
The title product was prepared from 3-phenoxyphenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (79%, colourless oil). HPLC-MS: m/z=320.1 (M+1); Rt: 5.16 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-e85b1339889e4b08ae6bee14ab28be75 |
| Source note | uspto-grants-2007_10 |