HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-2-methylacetophenone → HCID 69519179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-2-methylacetophenone | HCID 70133 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | HCID 69519179 | HCID 69519179 | — |
Reaction Steps
The title product was prepared from 4′-hydroxy-2′-methylacetophenone and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (76%, white crystals). HPLC-MS: m/z=284.2 (M+1); Rt: 3.95 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-d73068c2275a491ca393335511f4e8a6 |
| Source note | uspto-grants-2007_10 |