HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid benzo[d]isoxazol-3-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | HCID 178518983 | HCID 178518983 | — |
| Product | Methyl-phenyl-carbamic Acid benzo[d]isoxazol-3-yl Ester | HCID 69519226 | — |
Reaction Steps
The title product was prepared from benzo[d]isoxazol-3-ol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (53%, colorless oil). HPLC-MS: m/z=291.1 (M+23); Rt: 4.05 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-afb228d82c1f4b3581cc5480ab2888d9 |
| Source note | uspto-grants-2007_10 |