HRID1179887

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID75994

1-Benzylpiperazine

C11H16N2

结构：O=C(Cl)Oc1ccc(Oc2ncc(C(F)(F)F)cc2Cl)cc1

HCID22047691

未命名化合物

PRODUCTS

生成物

结构：O=C(Oc1ccc(Oc2ncc(C(F)(F)F)cc2Cl)cc1)N1CCN(Cc2ccccc2)CC1

HCID69519493

未命名化合物

PROCEDURE

实验过程

The hydrochloride of the title compound was prepared from 4-(3-chloro-5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate and 1-benzyl-piperazine, yield 94%. White crystals; m.p. 111-113° C. (resolidifies) and 114-115° C.; HPLC-MS m/z=492 (M+H).

WORKUP

后处理

customm.p. 111-113° C. (resolidifies) and 114-115° C.