HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzylpiperazine → HCID 69519493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Reactant | 4-(3-Chloro-5-trifluoromethylpyridin-2-yloxy)-phenyl chloroformate | HCID 22047691 | — |
| Product | HCID 69519493 | HCID 69519493 | — |
Reaction Steps
The hydrochloride of the title compound was prepared from 4-(3-chloro-5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate and 1-benzyl-piperazine, yield 94%. White crystals; m.p. 111-113° C. (resolidifies) and 114-115° C.; HPLC-MS m/z=492 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-eae060e0945e48a184c23f9b860d3977 |
| Source note | uspto-grants-2007_10 |