HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-acetyl-pyrazol-1-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | 1-(1-Hydroxy-1H-pyrazol-4-yl)ethanone | HCID 22047913 | — |
| Product | Methyl-phenyl-carbamic Acid 4-acetyl-pyrazol-1-yl Ester | HCID 69518094 | — |
Reaction Steps
The title compound was prepared from 1-hydroxy-4-acetylpyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (89%, oil).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-d622623ef6714d079d2be0b50f9252f2 |
| Source note | uspto-grants-2007_10 |