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HRID1179961

反应详情

EQUATION

反应方程式

HRID 1179961 的结构方程式

REACTANTS

反应物

3
结构：[Br-].[K+]
HCID253877

Potassium bromide

BrK

结构：c1cnc(N2CCNCC2)cn1
HCID2734639

1-Piperazinylpyrazine

C8H12N4

结构：O=C(Cl)Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1
HCID22047762

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1)N1CCN(c2cnccn2)CC1
HCID69519388

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate and 1-(pyrazin-2-yl)-piperazine White crystals, m.p. 160-161° C.; HPLC-MS: m/z=446 (M+1) at Rt=4.0 min.; 1H NMR (DMSO-d6): δ 8.60-8.57 (m, 1H), 8.39-8.36 (m, 1H), 8.27-8.22 (dd-like, 1H), 8.14-8.11 (m, 1H) 7.91-7.87 (d-like, 1H), 7.29-7.21 (m, 5H), 3.80-3.64 (br, 6H), 3.64-3.50 (br, 2H); IR (KBr): ν 1737, 1714 (C═O) cm−1.