HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidinemethanol → 4-Hydroxymethyl-piperidine-1-carboxylic Acid 4-(2-cyclohexyl-acetylamino)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidinemethanol | HCID 420771 | — |
| Reactant | 4-(2-Cyclohexyl-acetylamino)-phenyl chloroformate | HCID 22047886 | — |
| Product | 4-Hydroxymethyl-piperidine-1-carboxylic Acid 4-(2-cyclohexyl-acetylamino)-phenyl Ester | HCID 69518566 | — |
Reaction Steps
The title compound was prepared from 4-(2-cyclohexyl-acetylamino)-phenyl chloroformate and 4-hydroxymethyl-piperidine, preparative HPLC (Method C) (37%, off-white crystals). HPLC-MS m/z=375.2 (M+1), Rt: 3.41 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-9b01e2323bb7451ea67b11b7c7832e66 |
| Source note | uspto-grants-2007_10 |