HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(5-Trifluoromethylpyridin-2-yloxy)-phenyl chloroformate → HCID 69518109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(5-Trifluoromethylpyridin-2-yloxy)-phenyl chloroformate | HCID 22047762 | — |
| Reactant | HCID 45791934 | HCID 45791934 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69518109 | HCID 69518109 | — |
Reaction Steps
The title product was prepared from isopropyl-methyl-piperidin-4-yl-amine, dihydrochloride and 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate; dimethylformamide as solvent, preparative HPLC (method C) (77%, light yellow oil). HPLC-MS m/z=438.3 (M+1), Rt: 2.77 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-1872073473df436db8b131e6987c864a |
| Source note | uspto-grants-2007_10 |