HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methyl-4-anisidine → 4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenyl N-(4-methoxyphenyl)-N-methylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methyl-4-anisidine | HCID 22250 | — |
| Reactant | 4-(5-Trifluoromethylpyridin-2-yloxy)-phenyl chloroformate | HCID 22047762 | — |
| Product | 4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenyl N-(4-methoxyphenyl)-N-methylcarbamate | HCID 23635633 | — |
Reaction Steps
The title product was prepared from N-methyl-p-anisidine and 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate, preparative HPLC (method C) (61%, off-white crystals). HPLC-MS m/z=419.2 (M+1), Rt: 4.67 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-60df9c33a4c54ed096c21991a6c9da7c |
| Source note | uspto-grants-2007_10 |