3-(Methylaminomethyl)pyridine → HCID 69519738, compound

HRID 1180003Notes

Reaction equation

HRID 1180003 reaction equation
[CH3:1][NH:2][CH2:3][C:4]1[CH:5]=[N:6][CH:7]=[CH:8][CH:9]=1.O=C1CCC(=O)N1[O:17][C:18](=O)[C:19]1[CH:24]=[CH:23][C:22]([O:25][C:26](=[O:35])[N:27]([CH3:34])[C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)=[CH:21][CH:20]=1>>[CH3:1][N:2]([CH2:3][C:4]1[CH:5]=[N:6][CH:7]=[CH:8][CH:9]=1)[C:18]([C:19]1[CH:24]=[CH:23][C:22]([O:25][C:26](=[O:35])[N:27]([CH3:34])[C:28]2[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=2)=[CH:21][CH:20]=1)=[O:17]

Participants

3

Reactant 2

HCID 883933-(Methylaminomethyl)pyridineHCID 865892064-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester

Product 1

HCID 69519738HCID 69519738, compound

Procedure

The title product was prepared from methyl-pyridin-3-ylmethyl-amine and 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester. The crude product was subjected to preparative HPLC (method C) (48%, clear colourless oil). HPLC-MS m/z=376.2 (M+1), Rt: 2.37 min.

Sources & evidence

ORD record
ord-be55ea7366ce43cbb64806122011f022
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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