HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Methylaminomethyl)pyridine → HCID 69519738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Methylaminomethyl)pyridine | HCID 88393 | — |
| Reactant | 4-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester | HCID 86589206 | — |
| Product | HCID 69519738 | HCID 69519738 | — |
Reaction Steps
The title product was prepared from methyl-pyridin-3-ylmethyl-amine and 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester. The crude product was subjected to preparative HPLC (method C) (48%, clear colourless oil). HPLC-MS m/z=376.2 (M+1), Rt: 2.37 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-be55ea7366ce43cbb64806122011f022 |
| Source note | uspto-grants-2007_10 |