HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dimethylglutaric anhydride → HCID 22047706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dimethylglutaric anhydride | HCID 77813 | — |
| Reactant | HCID 69465626 | HCID 69465626 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22047706 | HCID 22047706 | — |
Reaction Steps
A solution of methyl-phenyl-carbamic acid 5-amino-pyridin-2-yl ester (243 mg, 1.00 mmol) and 3,3-dimethylglutaric anhydride (142 mg, 1.00 mmol) in dichloromethane (10 mL) was stirred at room temperature for 48 hours. Evaporation of the solvent yielded the title compound as a thick oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-8700b09099214e8eb2d34b59112d4302 |
| Source note | uspto-grants-2007_10 |