HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethylsuccinic anhydride → HCID 22047738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethylsuccinic anhydride | HCID 87067 | — |
| Reactant | HCID 69465626 | HCID 69465626 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22047738 | HCID 22047738 | — |
Reaction Steps
A solution of methyl-phenyl-carbamic acid 5-amino-pyridin-2-yl ester (0.49 g, 2.00 mmol) and 2,2-dimethylsuccinic anhydride (0.26 g, 2.00 mmol) in dichloromethane (10 mL) was stirred at room temperature overnight. Evaporation of the solvent in vacuo yielded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-85d85f88b9204af6b51e56998d5ec9bb |
| Source note | uspto-grants-2007_10 |