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HRID1180051

反应详情

EQUATION

反应方程式

HRID 1180051 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：Cl.On1ccnc1
HCID10313128

未命名化合物

结构：CN(C(=O)Oc1ccc(CO)cc1)c1ccccc1
HCID69518671

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(COn2ccnc2)cc1)c1ccccc1
HCID69519595

未命名化合物

收率 87%

PROCEDURE

实验过程

The title compound was prepared as its TFA salt in 87% yield as a solid using methyl-phenyl-carbamic acid 4-hydroxymethyl-phenyl ester and 1-hydroxyimidazole, hydrochloride. 1H NMR (400 MHz; CDCl3): δ 3.42 (br s, 3H), 5.21 (s, 2H), 6.95 (s, 1H), 7.16-7.45 (m, 10H), 8.28 (br s, 1H); HPLC-MS: m/z=324.1 (M+1); Rt=1.92 min.